Food Hormone balance 134 (2012) 696–703
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Food Hormone balance
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Characterisation of calamansi (Citrus microcarpa). Part II: Volatiles, physicochemical properties and non-volatiles in the juice
Mun Wai Cheong a, Danping Zhu a, Jingting Sng a, Shao Quan Liu a, Weibiao Zhou a, Philip Curran m, Bin Yu b, ⇑
a
w
Food Scientific research and Technology Programme, Office of Biochemistry, National University of Singapore, Science Drive 2, Singapore 117543, Singapore Firmenich Asia Pte., Limited., 10 Tuas West Street, Singapore 638377, Singapore
a r t i c l at the
i in f o
Article record:
Received 1 November 2011
Received in revised type 6 February 2012
Approved 22 Feb 2012
Available on the web 2 03 2012
Keywords:
Calamansi (Citrus microcarpa)
Juice
Volatile
Glucose
Organic acid solution
Phenolic acid solution
a w s big t r a c to
Calamansi drinks from 3 countries (Malaysia, the Korea and Vietnam) were characterized through measuring volatiles, physicochemical properties and non-volatiles (sugars, organic acids and phenolic acids). The volatile aspects of manually squashed calamansi juices were removed using dichloromethane and headspace solid-phase microextraction, and then analysed using gas chromatography–mass spectrometry/flame ionisation detector, respectively. A total of 60 volatile chemical substances were identiп¬Ѓed. The outcomes indicated the Vietnam calamansi juice contained the highest amount of volatiles. Two principal components extracted from principal component analysis (PCA) represented fifth there’s 89. 65% in the cumulative total variations of the volatiles. Among the list of non-volatile components, these 3 calamansi state of mind could be, at some level, differentiated in respect to fructose and blood sugar concentrations. Consequently, this analyze of calamansi juices could lead to a better understanding of calamansi fruits. Г“ 2012 Elsevier Ltd. All rights reserved.
1 . Introduction
For many centuries, citrus fruit juice has become valued as one of the healthiest and many consumed beverages, not only because of high nutritional C content, but likewise its special aroma and taste (Rouseff, Perez-Cacho, & Jabalpurwala, 2009). Besides common citrus fruits (i. e., orange, citrus and lime), exotic citrus fruits such as Pontianak lemon (Citrus nobilis var. microcarpa) from Indonesia, Mosambi (Citrus sinensis var. mosambi) from India and Dalandan (Citrus reticulata) from your Philippines, have got attracted very much attention (Dharmawan, Kasapis, Curran, & Johnson, 2007; Fischer, Grab, & Schieberle, 2008). Calamansi (Citrus microcarpa) juice has the mix of a sweet mandarin-like aroma with a zesty taste of lime, a slightly peel-like note of fruit and a touch of acidic astringency. It is commonly used being a seasoning in food, and it is also often used as a flavouring or as a food additive to boost iron ingestion. Our materials search indicated that, as of yet, there include only been four reports on calamansi juice (Nisperos-Carriedo, Baldwin, Moshonas, & Shaw, 1992; Takeuchi, Ubukata, Hanafusa, Hayashi, & Hashimoto, 2006; Wang, Chuang, & Ku, 2007; Por mi parte & Lin, 2004). By an synthetic perspective, the measurement of volatiles in citrus juice still remains a challenge. For instance , to preserve the authentic fragrant profile of citrus juice during extraction, it is ⇑ Corresponding publisher.
E-mail treat: bin. [email protected]п¬Ѓrmenich. com (B. Yu).
0308-8146/$ - observe front subject Г“ 2012 Elsevier Ltd. All legal rights reserved. http://dx.doi.org/10.1016/j.foodchem.2012.02.139
virtually extremely hard to obtain a substantial aroma mixture recovery (Dunn, Philips, & van Bronswijk, 1997). This is certainly partly because of the complex matrix and a restricted amount of volatile ingredients present in lemon or lime juice. Additionally to various microbe and enzyme activities, appealing yet volatile aroma compounds are easily altered while some off-flavour compounds are also quickly formed during extraction (Perez-Cacho & Rouseff, 2008). In...
References: Barboni, To., Luro, Farreneheit., Chiaramonti, And., Desjobert, T. M., Muselli, A., & Costa, J. (2009).
Bazemore, R., Goodner, K., & Rouseff, L. (1999). Volatiles from unpasteurized and
exceedingly heated lemon juice analyzed with sound phase microextraction and
Bazemore, R., Rouseff, R., & Naim, M. (2003). Linalool in orange colored juice. Origin and
thermal stability
Belingheri, L., Pauly, G., & Gleizes, Meters. (1991). Separating of limonene and selinene
cyclases by simply ion chromatography
Bocco, A., Cuvelier, M. E., Richard, H., & Berset, C. (1998). Antioxidant activity and
phenolic composition of Citrus peel and seed components
Food Chemistry, 46, 2123–2129.
Boccorh, R. K., Paterson, A., & Piggott, T. R. (1998). Factors influencing quantities of
sugars and organic acids in blackcurrant concentrates
Cheong, M. W., Chong, Unces. S., Liu, S. Queen., Zhou, T. B., Curran, P., & Yu, B. (2012).
Dharmawan, J., Kasapis, S., Curran, P., & Johnson, L. R. (2007). Characterization of
volatile ingredients in picked citrus fruits from Asia
Dunn, J. G., Philips, D., & van Bronswijk, W. (1997). An exercise to illustrate the
importance of test preparation in chemical evaluation
Education, 74(10), 1188–1190.
El-Sayed, A. Meters. (2011). The Pherobase: Database of pest phermones and
semiochemicals.
floral-taxa-compounds-index. php> (17 December 2011).
Fischer, A., Grab, T., & Schieberle, P. (2008). Characterisation of the extremely odouractive substances in a peel oil extract from Pontianak oranges (Citrus nobilis
Lour
Gattuso, G., Barreca, G., Gargiulli, C., Leuzzi, U., & Caristi, C. (2007). Flavonoid
make up of Lemon or lime juice
Hagerman, A. E., & Nicholson, R. D. (1982). Top of the line liquid
chromatographic determination of hydroxycinnamic acids in the maize
mesocotyl. Journal of Farming and Meals Chemistry, 30(6), 1098–1102.
Jouquand, C., & Chandler, C. (2008). A sensory and chemical analysis of refreshing
strawberries more than harvest date ranges and periods reveals factors that have an effect on eating
Kafkas, E., Ercisli, S., Kemal, K. D., Baydar, T., & Yilmaz, H. (2009). Chemical
make up of blood vessels orange varieties from Turkey: A comparative study.
Karadeniz, F. (2004). Main organic acid distribution of authentic citrus fruit drinks in
Turkey
Kelebek, They would. (2010). All kinds of sugar, organic acids, phenolic disposition and antioxidant
activity of grapefruit (Citrus paradisi) cultivars cultivated in Chicken
Kelebek, L., Canbas, A., & Selli, S. (2008). Determination of phenolic structure
and antioxidant capacity of blood lemon juices extracted from cvs
Sanguinello (Citrus sinensis (L. ) Osbeck) cultivated in Poultry. Food Biochemistry, 107(4),
1710–1716.
Kelebek, H., & Selli, S. (2011). Determination of volatile, phenolic, organic acid solution and
sugar components in a Turkish cv
juice. Record of the Technology of Foodstuff and Culture, 91(10), 1855–1862.
Kelebek, They would., Selli, S., Canbas, A., & Cabaroglu, T. (2009). HPLC willpower of
organic and natural acids, all kinds of sugar, phenolic arrangement and antioxidant capacity of orange
Moshonas, M. G., & Shaw, P. At the. (1994). Quantitative-determination of 46 volatile
constituents in new, unpasteurized orange colored juices using dynamic headspace
gas-chromatography. Record of Agricultural and Foodstuff Chemistry, 42(7),
1525–1528.
Moshonas, M. G., & Shaw, P. Electronic. (1996). Volatile components of calamondin peel essential oil.
Journal of Agricultural and Food Chemistry, 44, 1105–1107.
Nardini, M., Cirillo, Elizabeth., Natella, Farrenheit., Mencarelli, D., Comisso, A., & Scaccini, C. (2002).
Nisperos-Carriedo, Meters. O., Baldwin, E. A., Moshonas, Meters. G., & Shaw, P. E. (1992).
Journal of Agricultural and Food Chemistry, 40, 2464–2466.
Nour, V., Trandafir, My spouse and i., & Ionica, M. At the. (2010). HPLC organic acidity analysis in different
citrus juices under turned phase conditions
Peleg, They would., Naim, M., Rouseff, Ur. L., & Zehavi, U. (1991). Syndication of destined and totally free
phenolic stomach acids in oranges (Citrus sinensis) and Grapefruits (Citrus paradisi).
Peleg, L., Naim, Meters., Zehavi, U., Rouseff, 3rd there’s r. L., & Nagy, H. (1992). Pathways of 4vinylguaiacol formation from ferulic chemical p in model solutions of orange drink.
Perez-Cacho, S. R., & Rouseff, Ur. L. (2008). Fresh squashed orange juice odor: A
review
PГ©rez-LГіpez, A., Saura, D., Lorente, J., & Carbonell-Barrachina, ГЃ. (2006). Limonene,
linalool, a-terpineol, and terpinen-4-ol as quality control parameters in
Rapisarda, P., Carollo, G., Fallico, B., Tomaselli, F., & Maccarone, Elizabeth. (1998).
Rouseff, R. M., Perez-Cacho, P. R., & Jabalpurwala, N. (2009). Historical review of citrus
flavor exploration during the past 100 years